HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-bromo-2-chloro-6-trifluoromethyl-1H-benzoimidazole → HCID 178519686, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-bromo-2-chloro-6-trifluoromethyl-1H-benzoimidazole | HCID 11594585 | — |
| Reactant | 2-(1-piperazinyl)-3-Pyridinemethanol | HCID 67400406 | — |
| Product | HCID 178519686 | HCID 178519686 | — |
Reaction Steps
(2-piperazin-1-ylpyridin-3-yl)methanol (0.48 g, 2.5 mmol, Example 46a) reacted with 4-bromo-2-chloro-6-trifluoromethyl-1H-benzoimidazole (0.60 g, 2 mmol, Example 6b) under the conditions of Example 3c to give the title compound as a white amorphous solid. MS (ESI, pos. ion) m/z: 456 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08026241B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-9f667f4066d84bdd8431b7ef1553fa46 |
| Source note | uspto-grants-2011_09 |