HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 178478308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 6-bromo-3H-imidazo[4,5-b]pyridin-2-ol | HCID 1924413 | — |
| Product | HCID 178478308 | HCID 178478308 | — |
Reaction Steps
The pyridin-2-one from step (a) above (1 g, 4.7 mmol) reacted with POCl3 under the conditions of Example 1c to give the title compound as a brown solid. MS (ESI, pos. ion) m/z: 232 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08026241B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-f6d6b936e41941aab3cdef5e15340b0b |
| Source note | uspto-grants-2011_09 |