HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 3,5-Diethoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3,5-Dihydroxybenzaldehyde | HCID 94365 | — |
| Reactant | 3-Ethoxy-4-methylbenzaldehyde | HCID 25242058 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 3,5-Diethoxybenzaldehyde | HCID 22608616 | — |
Reaction Steps
The title compound was prepared analogously to 3-ethoxy-4-methyl-benzaldehyde (intermediate E10, vide infra) by reaction of 3,5-dihydroxybenzaldehyde with ethyl iodide in DMF using K2CO3 as base.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08026255B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-67ab65cfdd204b448352cd73cb01b4fe |
| Source note | uspto-grants-2011_09 |