Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Allyl bromide → 3-Allyloxy-4-methoxybenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Allyl bromide | HCID 7841 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | Isovanillin | HCID 12127 | — |
| 반응물 | 3-Ethoxy-4-methylbenzaldehyde | HCID 25242058 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 3-Allyloxy-4-methoxybenzaldehyde | HCID 534148 | — |
반응 단계
The title compound was prepared analogously to 3-ethoxy-4-methyl-benzaldehyde (intermediate E10) by reaction of 3-hydroxy-4-methoxy-benzaldehyde with allylbromide in DMF using K2CO3 as base (see also A. W. White, R. Almassy, A. H. Calvert, N. J. Curtin, R. J. Griffin, Z. Hostomsky, K. Maegley, D. R. Newell, S. Srinivasan and B. T. Golding J. Med. Chem. 2000, 43, 4084-4097).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08026255B2 |
| 출처 데이터셋 | uspto-grants-2011_09 |
| ORD ID | ord-9b2a613a32ef49a39cfc5cedf03cc61e |
| 출처 메모 | uspto-grants-2011_09 |