HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-3-ethoxybenzaldehyde → HCID 67399435, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-3-ethoxybenzaldehyde | HCID 54775642 | — |
| Reactant | HCID 67398466 | HCID 67398466 | — |
| Reactant | HCID 67401550 | HCID 67401550 | — |
| Product | HCID 67399435 | HCID 67399435 | — |
Reaction Steps
The title compound was prepared in analogy to the synthesis of 2-[1-(3-ethoxy-4-methyl-benzyl)-piperidin-4-ylamino]-isonicotinonitrile (example 189) from 2-(piperidin-4-ylamino)-isonicotinonitrile dihydrochloride (intermediate B15) and 4-chloro-3-ethoxy-benzaldehyde (intermediate E2) in a yield of 3.8 mg (6%). MS (ISP): 371.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08026255B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-965a8abe66c44cc5bf51c6fef36623b8 |
| Source note | uspto-grants-2011_09 |