HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenothiazine → Hydroxyethylimidazole Acrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenothiazine | HCID 7108 | — |
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | 4-Methoxyphenol | HCID 9015 | — |
| Reactant | 2-(1H-imidazol-2-yl)ethan-1-ol | HCID 15016080 | — |
| Product | Hydroxyethylimidazole Acrylate | HCID 67412270 | — |
Reaction Steps
At a temperature of 60° C., methyl acrylate (MA) and hydroxyethylimidazole (HEI) in a molar ratio of 5:1 were heated in the presence of 50 ppm of phenothiazine, 500 ppm of hydroquinone monomethyl ether and 1.25 mol % of a catalyst (based on hydroxyethylimidazole) for 5 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08026374B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-9bd0b1b7868b45179706b848c10dc493 |
| Source note | uspto-grants-2011_09 |