HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Chloromethyl)-5-[3-(trifluoromethyl)phenyl]-1,2,4-oxadiazole → HCID 57800067, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Chloromethyl)-5-[3-(trifluoromethyl)phenyl]-1,2,4-oxadiazole | HCID 2736622 | — |
| Reactant | HCID 67404000 | HCID 67404000 | — |
| Product | HCID 57800067 | HCID 57800067 | — |
Reaction Steps
Synthesized as described in Example 4 from 4-chloro-2-(3,3,3-trifluoropropyl)-1H-indole-5-carbonitrile and 3-(chloromethyl)-5-[3-(trifluoromethyl)phenyl]-1,2,4-oxadiazole: 1H NMR (400 MHz, CDCl3) δ 8.31 (s, 1 H), 8.23 (d, J=7.8 Hz, 1 H), 7.86 (d, J=7.9 Hz, 1H), 7.67 (dd, J=7.8 Hz, 1 H), 7.45 (s, 2 H), 6.56 (s, 1 H), 5.45 (s, 2 H), 3.27 (t, 2 H), 2.89-2.61 (m, 2 H); MS (ES) m/z 499 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08026262B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-7f45cd5c71e84fe6955c21e83ffa4c4a |
| Source note | uspto-grants-2011_09 |