HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-methyl-4-(trifluoromethyl)-1H-indole-5-carbonitrile → HCID 67406398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-methyl-4-(trifluoromethyl)-1H-indole-5-carbonitrile | HCID 53309346 | — |
| Reactant | HCID 67404843 | HCID 67404843 | — |
| Product | HCID 67406398 | HCID 67406398 | — |
Reaction Steps
Synthesized as described in Example 4 using 2-methyl-4-(trifluoromethyl)-1H-indole-5-carbonitrile (Example 120) and 2-bromoethyl-4-fluorophenylether: 1H NMR (400 MHz, CDCl3) δ 7.57 (d, J=8.5 Hz, 1H), 7.52 (d, J=8.5 Hz, 1H), 6.92 (t, J=8.6 Hz, 2H), 6.69 (m, 2H), 6.59 (s, 1H), 4.53 (t, J=5.3 Hz, 2H), 4.20 (t, J=5.3 Hz, 2H), 2.57 (s, 3H): MS (ES) m/z 363 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08026262B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-b849049283394cf99f5b89efe0c11a40 |
| Source note | uspto-grants-2011_09 |