HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-4-chloroaniline → 7-bromo-5-chloro-1H-indole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-4-chloroaniline | HCID 70110 | — |
| Reactant | 7-Bromo-5-(trifluoromethyl)-1H-indole | HCID 57546135 | — |
| Product | 7-bromo-5-chloro-1H-indole | HCID 24729504 | — |
Reaction Steps
Made from 2-bromo-4-chloroaniline using the method for 7-bromo-5-(trifluoromethyl)-1H-indole. 1H-NMR (CDCl3, 400 MHz) δ 8.32 (bs, 1H), 7.55 (d, J=1.2 Hz, 1H), 7.55 (d, J=1.8 Hz, 1H), 7.27 (t, J=3.0 Hz, 1H), 6.56 (dd, J=3.3, 2.3 Hz, 1H). LC/MS (HPLC method 4): tR=3.07 min, 229.95(MH)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08026257B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-e040ca7804184ab1b9c3e5314c2074ef |
| Source note | uspto-grants-2011_09 |