HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Ethoxypyridin-3-amine → (6-Ethoxy-pyridin-3-yl)-isopropyl-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Ethoxypyridin-3-amine | HCID 3040301 | — |
| Reactant | 6-chloro-N-(propan-2-yl)pyridin-3-amine | HCID 58957920 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | (6-Ethoxy-pyridin-3-yl)-isopropyl-amine | HCID 58957938 | — |
Reaction Steps
Following the procedure described for Preparation 2(A), 6-ethoxy-pyridin-3-ylamine (10 g, 72.4 mmol) was reacted with acetone (4.8 mL) to provide 11.18 g of (6-ethoxy-pyridin-3-yl)-isopropyl-amine. 1H NMR (CD3OD) δ 7.48 (d, 1H), 7.11 (dd, 1H), 6.61 (d, 1H), 4.14 (q, 2H), 3.48 (m, 1H), 1.32 (t, 3H), 1.14 (d, 6H); MS 181.3 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07265104B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-af56b0cadabd461e9d288e7bc1bc33a7 |
| Source note | uspto-grants-2007_09 |