反应详情

温度

65 °C

To a solution of methyl cyclohexane carboxylate (12 g, 83.9 mmol) in MeOH (50 mL) was added hydrazine (5.3 mL, 1.67 mol). The reaction mixture was heated at 65° C. overnight. The reaction mixture was cooled to room temperature and the resultant solid was collected by filtration and was dried in vacuo to give 4.0 g of cyclohexanecarboxylic acid hydrazide.

1. temperatureThe reaction mixture was cooled to room temperature
2. filtrationthe resultant solid was collected by filtration
3. customwas dried in vacuo