HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22248599, compound → HCID 22248483, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22248599 | HCID 22248599 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22248483 | HCID 22248483 | 195.3% |
Reaction Steps
After then dissolving 50 mg of the 3-benzyloxycarbonyl-8-(2-fluorophenyl)-7-oxo-3-azabicyclo[4.3.0]nonane in 30 ml of methanol, 100 mg of 10% palladium-carbon was added and the mixture was stirred for 4 days at room temperature under a hydrogen atmosphere (1 atm). The reaction mixture was filtered and the filtrate was distilled off under reduced pressure to obtain 62 mg of 8-(2-fluorophenyl)-7-oxo-3-azabicyclo[4.3.0]nonane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07265108B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-1357baf68a54438a8a8df704e5714ac9 |
| Source note | uspto-grants-2007_09 |