HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl isocyanate → HCID 22260529, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl isocyanate | HCID 7672 | — |
| Reactant | 4-Methylmorpholine | HCID 7972 | — |
| Reactant | HCID 22260424 | HCID 22260424 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 22260529 | HCID 22260529 | — |
Reaction Steps
The title compound is prepared from morpholine-4-carboxylic acid [1-(4-cyano-piperidin-4-ylcarbamoyl)-3,3-dimethyl-butyl]-amide hydrochloride and phenyl isocyanate in the presence of a tertiary amine base such as N-methylmorpholine in a solvent such as methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07265132B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-f40c1d1187434b7b97a5ec5d79b7f633 |
| Source note | uspto-grants-2007_09 |