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HRID915348

反应详情

EQUATION

反应方程式

HRID 915348 的结构方程式

REACTANTS

反应物

1
结构：CCOC(=O)c1[nH]c2ccc(-n3cccc3)cc2c1-c1ccccc1
HCID69340873

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O)c1[nH]c2ccc(-n3cccc3)cc2c1-c1ccccc1
HCID11392466

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

The title compound was prepared from ethyl 3-phenyl-5-(1H-pyrrol-1-yl)-1H-indole-2-carboxylate followed the procedure of Example 1 Step 4 as an off-white solid: 1H NMR (DMSO-6) δ 6.21 (s, 2 H), 7.20 (s, 2 H), 7.20-7.60 (m, 7 H), 11.92 (s, 1H), 13.0 (br s, 1 H); MS (ESI) m/z 303 (MH+); MS (ESI) m/z 301 ([M-H]−); HRMS calcd for C19H15N2O2: 303.1134; found (ESI+): 303.1124; Anal. calcd for C19H14N2O2.1.3 H2O: C, 70.06; H, 5.13; N, 8.60. Found: C, 70.22; H, 5.08; N, 8.21.