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HRID915444

反应详情

EQUATION

反应方程式

HRID 915444 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[Cs+].[Cs+]
HCID10796

Cesium carbonate

CCs2O3

结构：CC(C)(C)OC(=O)CBr
HCID79177

Acetic acid, bromo-, 1,1-dimethylethyl ester

C6H11BrO2

结构：Cc1cc(OCc2ccccc2)cc2[nH]ccc12
HCID69280240

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(OCc2ccccc2)cc2c1ccn2CC(=O)OC(C)(C)C
HCID69280223

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

In analogy to the procedure described in example 1 c], 6-benzyloxy-4-methyl-1H-indole was reacted with bromo-acetic acid tert-butyl ester in the presence of cesium carbonate in DMF to obtain (6-benzyloxy-4-methyl-indol-1-yl)-acetic acid tert-butyl ester as yellow oil.