HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Oxalate → HCID 178473087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Oxalate | HCID 7268 | — |
| Reactant | 4'-Fluoro-3'-(trifluoromethyl)acetophenone | HCID 605678 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Product | HCID 178473087 | HCID 178473087 | — |
Reaction Steps
In analogy to the procedure described for example 11 a], 1-(4-fluoro-3-trifluoromethyl-phenyl)-ethanone was reacted with diethyl oxalate in the presence of metallic sodium to give (Z)-4-(4-fluoro-3-trifluoromethyl-phenyl)-2-hydroxy-4-oxo-but-2-enoic acid ethyl ester as colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07265149B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-09b5c003d8cf4b0bb09515f0755ba42c |
| Source note | uspto-grants-2007_09 |