Azobisisobutyronitrile → HCID 86601183, compound

Participants

Reaction Steps

10 g of t-butylacrylate, 4 g of acrylic acid, 6 g of N-isopropylacrylamide and 0.4 g of AIBN were added to 200 g of PGMEA, and were then polymerized at 60° C. for 8 hours. After completion of the polymerization, the mixture was precipitated in ether, filtered, and dried in a vacuum to yield 17 g of poly(t-butylacrylate-acrylic acid-N-isopropylacrylamide) copolymer, as a white solid, represented by Formula 2 below:

Provenance & Evidence