HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → Sodium Behenate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Docosanoic Acid | HCID 8215 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | tert-Butanol | HCID 6386 | — |
| Product | Sodium Behenate | HCID 23668838 | — |
Reaction Steps
Behenic acid (being Edenor C22-85R, manufactured by Henckel Corp.) of 87.6 kg, 423 L of distilled water, 49.2 L of sodium hydroxide at a concentration of 5 mol/L and 120 L of t-butylalcohol were mixed, and the mixture was allowed react at 75° C. while stirred for 1 hour, resulting in preparation of a sodium behenate solution. Separately, 206.2 L (pH of 4.0) of an aqueous solution containing 40.4 kg of silver nitrate were prepared and temporarily stored at 10° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07267934B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-3df6fe8b73724565bcd6ae0698441fb1 |
| Source note | uspto-grants-2007_09 |