HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-5-methylpyridine → 1-(2-Fluoro-5-methylpyridin-3-yl)methanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-5-methylpyridine | HCID 2774635 | — |
| Reactant | HCID 66732973 | HCID 66732973 | — |
| Product | 1-(2-Fluoro-5-methylpyridin-3-yl)methanamine | HCID 53426950 | — |
Reaction Steps
(2-fluoro-5-methylpyridin-3-yl)methanamine (2-e) was prepared by the same synthetic route as that of (2-g) but utilizing the commercially available 2-fluoro-5-methylpyridine (2-c) as a starting material; 1H NMR (500 MHz, DMSO-d6) δ 8.65 (bs, 3 H), 8.07 (d, 1 H, J=1.0 Hz), 8.01 (dd, 1 H, J=15.5, 3.0 Hz), 4.02 (s, 2 H), 2.30 (s, 3 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07268153B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-60f5d81a153940909782a4e260e2896c |
| Source note | uspto-grants-2007_09 |