Methanesulfonyl chloride → HCID 11441550, compound

Participants

Reaction Steps

The title compound was prepared from 1-(4-nitro-benzyl)-3-phenyl-1H-indole indolecarboxylic acid ethyl ester and methanesulfonyl chloride followed the procedure of Example 3 Step 2 as an off-white solid: 1H NMR (DMSO-d6) δ 2.94 (s, 3H), 5.80 (s, 2H), 7.05-7.15 (m, 5H), 7.31-7.38 (m, 2H), 7.43-7.47 (m, 5H), 7.62 (d, J=8.4 Hz, 1H), 9.68 (br s, 1H), 12.87 (br s, 1H); MS (ESI) m/z 419 ([M−H]−); HRMS calcd for C23H19N2O4S: 419.1068; found (ESI−): 419.1074.

Provenance & Evidence