HCID 12143941, compound → HCID 22136257, compound

HRID 916222Notes

Reaction equation

HRID 916222 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([CH3:8])[CH:5]=[C:4](C)[C:3]=1N1CCCC2C(=O)N(C)NC1=2.[Cl:21][C:22]1[CH:27]=[C:26]([Cl:28])[CH:25]=[CH:24][C:23]=1[N:29]1[CH2:34][CH2:33][CH2:32][C:31]2[C:35](=[O:39])[N:36]([CH3:38])[NH:37][C:30]1=2>>[ClH:1].[Cl:21][C:22]1[CH:27]=[C:26]([Cl:28])[CH:25]=[CH:24][C:23]=1[N:29]1[CH2:34][CH2:33][CH2:32][C:31]2=[C:35]([O:39][CH:2]([CH2:7][CH2:6][CH3:8])[CH2:3][CH2:4][CH3:5])[N:36]([CH3:38])[N:37]=[C:30]12

Participants

3

Reactant 2

HCID 12143941HCID 12143941, compoundHCID 221362907-(2,4-Dichlorophenyl)-2-methyl-1,2,4,5,6,7-hexahydropyrazolo[3,4-b]pyridin-3-one

Product 1

HCID 22136257HCID 22136257, compound

Procedure

Example 12b was prepared according to the procedure described in Example 12a, except that 7-(2-chloro-4,6-dimethylphenyl)-2-methyl-1,2,4,5,6,7-hexahydropyrazolo[3,4-b]pyridin-3-one was replaced by 7-(2,4-dichlorophenyl)-2-methyl-1,2,4,5,6,7-hexahydropyrazolo[3,4-b]pyridin-3-one.

Workup

  1. customExample 12b was prepared

Sources & evidence

ORD record
ord-90bcd4cc692a4ceb89f884ed3372ea3f
Source dataset
uspto-grants-2007_09
Patent number
US07268146B2

Reaction notes

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