HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyaniline → 2-Methoxyformanilide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyaniline | HCID 7000 | — |
| Reactant | 2-Nitroanisole | HCID 7048 | — |
| Catalyst | HCID 178419084 | HCID 178419084 | — |
| Product | 2-Methoxyformanilide | HCID 243581 | 24.8% |
Reaction Steps
The procedure of Example 4 was repeated using o-nitroanisole (4 mmol, 0.55 g) as starting material and vanadium(v) oxide (2.3 mg) instead of sodium molybdate dihydrate. After 2.5 h at 90-95° C. a yield of 24.8% of o-formoanisidide was obtained. o-Anisidine (62.8%) was found to be the main product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07268255B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-bc26d3108f42421e9d4cda553a606bfd |
| Source note | uspto-grants-2007_09 |