HCID 69225857, compound → HCID 11515268, compound

Participants

Reaction Steps

159JP95C (12 mg, 0.038 mmol) and palladium (10 mg, 10 wt. % on activated carbon) in methanol (10 mL) were stirred for 3 days at rt under hydrogen atmosphere (balloon). The suspension was filtered through a pad of Celite, concentrated in vacuo and purification by preparative TLC (ethyl acetate/n-heptane, 1:4, 2× eluted) afforded the title compound (5.0 mg, 42%) as a colorless oil.

Provenance & Evidence