3,4-Diaminobenzoic acid → HCID 178524159, compound

HRID 916741Notes

Reaction equation

HRID 916741 reaction equation
F[C:2]1[CH:16]=[CH:15][C:5]([O:6][C:7]2[CH:14]=[CH:13][C:10]([CH:11]=O)=[CH:9][CH:8]=2)=[CH:4][CH:3]=1.[NH2:17][C:18]1[CH:19]=[C:20]([CH:24]=[CH:25][C:26]=1[NH2:27])[C:21]([OH:23])=[O:22].NC1C=C(C=CC=1N)C(N)=O>>[O:6]([C:7]1[CH:14]=[CH:13][C:10]([C:11]2[NH:27][C:26]3[CH:25]=[CH:24][C:20]([C:21]([OH:23])=[O:22])=[CH:19][C:18]=3[N:17]=2)=[CH:9][CH:8]=1)[C:5]1[CH:15]=[CH:16][CH:2]=[CH:3][CH:4]=1

Participants

4

Reactant 3

HCID 692633,4-Diaminobenzoic acidHCID 38568024-(4-Fluorophenoxy)benzaldehydeHCID 212178433,4-Diaminobenzamide

Product 1

HCID 178524159HCID 178524159, compound

Procedure

This compound was prepared according to the methods described in Example 22 and Scheme 3, substituting 4-phenoxybenzaldehyde for 4-(4-fluoro-phenoxy)-benzaldehyde, and 3,4-diaminobenzoic acid for 3,4-diaminobenzoic acid amide.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-7646f0aaaa6948eba3f9ab9fffa5d713
Source dataset
uspto-grants-2007_09
Patent number
US07271261B2

Reaction notes

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