HCID 69384227, compound → HCID 69385724, compound

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Reaction Steps

N-[3-({2-[4-(2-{[(2R)-2-(2,2-Dimethyl-4H-1,3-benzodioxin-6-yl)-2-hydroxyethyl]amino}ethyl)phenoxy]ethoxy}methyl)phenyl]urea (12 mg) in acetic acid (1.5 mL) and water (0.5 mL) was heated at 75° C. for 0.5 h. The solution was then concentrated in vacuo and azeotroped with MeOH to give the title compound (13 mg). LCMS RT=2.18 min. ES+ve 496 (MH)+

Provenance & Evidence