HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 69389155, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 69387393 | HCID 69387393 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 69389155 | HCID 69389155 | — |
Reaction Steps
A solution of tert-butyl{4-[3-(cyclopentylsulfinyl)phenyl]butoxy}diphenylsilane (690 mg) in dry THF (10 ml) was treated with a solution of tetra-n-butylammonium fluoride in THF (1M; 3 ml) and the resultant reaction mixture stirred at room temperature for 5 h prior to concentration in vacuo. The residue was purified by chromatography (SPE, Gradient between cyclohexane and EtOAc) to give the title compound. LCMS RT=2.64 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07271197B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-ec40f99142da467f9f42bfae2789d496 |
| Source note | uspto-grants-2007_09 |