Diethyl Ether → HCID 22493753, compound

HRID 916878Notes

Reaction equation

HRID 916878 reaction equation
[CH2:1]([N:5]1[C:9]([CH:10]=[O:11])=[CH:8][N:7]=[C:6]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH2:2][CH2:3][CH3:4].[CH2:18](OCC)C>>[CH2:1]([N:5]1[C:9]([CH:10]([OH:11])[CH3:18])=[CH:8][N:7]=[C:6]1[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH2:2][CH2:3][CH3:4]

Participants

3

Reactant 2

HCID 3283Diethyl EtherHCID 10633115HCID 10633115, compound

Product 1

HCID 22493753HCID 22493753, compound

Procedure

A solution of aldehyde 102 (230 mg) in diethyl ether (30 mL) is placed in a separatory funnel and treated with a solution of

Workup

  1. additiontreated with a solution of

Sources & evidence

ORD record
ord-66b429919ca5476eb0f61446191a3c44
Source dataset
uspto-grants-2007_09
Patent number
US07271270B2

Reaction notes

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