HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylmorpholine → 3-Methoxy-N-(7-methoxy-4-phenyl-thiazolo[5,4-c]pyridin-2-yl)-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylmorpholine | HCID 7972 | — |
| Reactant | 3-Methoxybenzoic Acid | HCID 11461 | — |
| Reactant | Methanaminium, N-((dimethylamino)(3H-1,2,3-triazolo(4,5-b)pyridin-3-yloxy)methylene)-N-methyl-, hexafluorophosphate(1-) (1:1) | HCID 9886157 | — |
| Reactant | 7-Methoxy-4-phenyl-thiazolo[5,4-c]pyridin-2-ylamine | HCID 86038474 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-Methoxy-N-(7-methoxy-4-phenyl-thiazolo[5,4-c]pyridin-2-yl)-benzamide | HCID 11502024 | — |
Reaction Steps
From 3-methoxybenzoic acid, HATU and N-methylmorpholine in THF, then treatment with 7-methoxy-4-phenyl-thiazolo[5,4-c]pyridin-2-ylamine. ES-MS m/e (%): 392 (M+H+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07273865B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-7627e79cbe074ce1b04f1ce975e397f8 |
| Source note | uspto-grants-2007_09 |