HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzyl bromide → HCID 69413663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzyl bromide | HCID 68021 | — |
| Reactant | HCID 18980505 | HCID 18980505 | — |
| Reactant | HCID 23105694 | HCID 23105694 | — |
| Product | HCID 69413663 | HCID 69413663 | — |
Reaction Steps
When reacting 2-dimethylaminomethyl-1-(3-methoxyphenyl)-cyclohexane-1,4-diol hydrochloride with 4-fluorobenzylbromide in accordance with AAV 7, (2,5-bis-(4-fluorobenzyloxy)-2-(3-methoxyphenyl)-cyclohexylmethyl]-dimethylamine was also obtained as a secondary product after chromatographic purification on silica gel, which was converted into the corresponding hydrochloride in the same way as in AAV 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07273952B2 |
| Source dataset | uspto-grants-2007_09 |
| ORD ID | ord-08c5a73b2a674f609c52f22a7e990943 |
| Source note | uspto-grants-2007_09 |