HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 12939990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Dimethylcarbamoyl Chloride | HCID 6598 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 5-chloro-N-methyl-1,3-benzothiazol-2-amine | HCID 2726858 | — |
| Product | HCID 12939990 | HCID 12939990 | — |
Reaction Steps
N,N-dimethylcarbamoylchloride (1.1g) and 5-chloro-2-methylaminobenzothiazole (2g) were dissolved in dimethylformamide (25ml) and the mixture was stirred while adding slowly sodiumhydride (0.44g, 55% oily) in a stream of nitrogen for an hour and maintaining the temperature below -5°C. After stirring 3 additional hours at the room temperature, the mixture was poured into water (100ml) and the precipitate was filtrated, washed and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03967950 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-93aeb2eedfd243db89beedaef9d512b2 |
| Source note | uspto-grants-1976_07 |