HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoprene → HCID 53632406, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoprene | HCID 6557 | — |
| Reactant | 2-Norbornene | HCID 10352 | — |
| Catalyst | Pyrogallol | HCID 1057 | — |
| Product | HCID 53632406 | HCID 53632406 | 38% |
Reaction Steps
A mixture of 715 g (7.6 M) of norbornene, 550 g (8.1 M) of isoprene and 2 g of pyrogallol was heated in a stainless steel autoclave at ca. 150° during 15 hours. An internal pressure of 20 atm. is thus reached. The reaction mixture was then distilled by means of a Vigreux column and yielded 467 g (yield 38%) of 5-methyl-tricyclo[6.2.1.02,7 ]undec-4-ene having b.p. 90°/10 Torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03968070 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-0f097907133c46d2b2b1976ea3a99738 |
| Source note | uspto-grants-1976_07 |