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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 917835Generated: October 29, 2026

Ethylene Glycol → HCID 131710010, compound

https://huagongshe.com/reaction/917835

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthylene GlycolHCID 174—
ReactantAcetoneHCID 180—
ReactantSodium HydroxideHCID 14798—
Reactant2,5-Dioxo-2,5-dihydrofuran-3-sulfonic acidHCID 12479880—
SolventWaterHCID 962—
ProductHCID 131710010HCID 131710010—

Reaction Conditions

Temperature80 °C

Reaction Steps

Sulfomaleic anhydride (20 gm) is mixed with 37.2 gm (0.6 mole) of ethylene glycol and heated at 80°C for 4 hours. A solution of 16 gm (0.4 mole) of sodium hydroxide in 75 ml of water is then added and the mixture heated at 80°C for 4 hours. The mixture is then mixed with acetone to precipitate trisodium α-hydroxyethoxy-β-sulfosuccinate, which is purified by repeated extractions with hot acetone to remove all ethylene glycol and water followed by filtration and drying in an oven.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS03968110
Source datasetuspto-grants-1976_07
ORD IDord-e1825c97161148b48b6786bb2dbbd595
Source noteuspto-grants-1976_07