HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → Mesitylene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | 1-(4-Methoxyphenyl)-2-phenyl-4,5,6,7-tetrahydroindole | HCID 13522538 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Mesitylene | HCID 7947 | — |
Reaction Steps
Following a procedure similar to that of Example 1D but using 63 g. of 1-(4-methoxyphenyl)-2-phenyl-4,5,6,7-tetrahydroindole and 18 g. of 10% palladium-on-charcoal in 600 ml. mesitylene (18 hours reflux) there was obtained, on recrystallization first from isopropyl alcohol and then from tetrahydrofuran-hexane, 58.5 g. of 1-(4-methoxyphenyl)-2-phenylindole; m.p. 141°-142°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03968121 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-8d60b5116c00491fa7432698c4cd8171 |
| Source note | uspto-grants-1976_07 |