Tert-Butylbenzene → HCID 23463452, compound

HRID 917928Notes

Reaction equation

HRID 917928 reaction equation
[C:1](Cl)(=[O:5])[CH2:2][CH2:3][CH3:4].[C:7]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)([CH3:10])([CH3:9])[CH3:8]>>[C:7]([C:11]1[CH:16]=[CH:15][C:14]([C:1](=[O:5])[CH2:2][CH2:3][CH3:4])=[CH:13][CH:12]=1)([CH3:10])([CH3:9])[CH3:8]

Participants

3

Reactant 2

HCID 7366Tert-ButylbenzeneHCID 8855Butyryl chloride

Product 1

HCID 23463452HCID 23463452, compound

Procedure

The procedure of Example 3 was followed for the reaction of 53g (0.5 mole) of butyryl chloride with 67g (0.5 mole) of tert-butyl benzene. Obtained after high vacuum concentration was 94g of a clear liquid. A VPC analysis indicated a pure product. Ir (film) 3.5 (s), 5.9 (s) microns; nmr (CDCl3) 7.65 (4H, center doublet of doublets), 2.9 (2H, t), 1.75 (2H, sextet), 1.3 (9H, s), 0.95 (3H, t) ppm.

Workup

  1. customObtained
  2. concentrationafter high vacuum concentration

Sources & evidence

ORD record
ord-2ca9d8267bc443429a64e5b0379d254d
Source dataset
uspto-grants-1976_07
Patent number
US03968168

Reaction notes

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