HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Pyridin-2-yl)propan-1-amine → HCID 178512789, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Pyridin-2-yl)propan-1-amine | HCID 3159614 | — |
| Reactant | S-methyl isothiourea hemisulfate | HCID 6604939 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178512789 | HCID 178512789 | — |
Reaction Steps
A solution of 2-(3-aminopropyl)pyridine (2.72 g) and S-methylthiouronium sulphate (2.78 g) in water (40 ml) is heated under reflux for 28 hours. The product isolated by the manner described in Example 1 was recrystallized from methanol, yielding 3-(2-pyridyl)propylguanidine sulphate, m.p. 185°-187°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03968216 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-6614860d3d4a42fabafd3169fbd7b679 |
| Source note | uspto-grants-1976_07 |