HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenylprop-2-En-1-Ol → HCID 53806082, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenylprop-2-En-1-Ol | HCID 308 | — |
| Reactant | Sesamol | HCID 68289 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 53806082 | HCID 53806082 | — |
Reaction Steps
The compounds of Category II may be prepared in the following manner: A mixture of sesamol and cinnamyl alcohol in aqueous formic acid is refluxed to yield 2-hydroxy-4,5-methylenedioxy-cinnamylbenzene. This intermediate is then etherified in conventional manner by reaction with an appropriate alkyl halide or alkyl sulphate to yield the desired compound. The synthesis is illustrated by the following formulas. ##EQU4##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03968234 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-0b9f686aec574a389fe2fffd9e7ef0cf |
| Source note | uspto-grants-1976_07 |