HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanethiol → HCID 178484946, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanethiol | HCID 878 | — |
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Methyl N,N'-dimethylcarbamimidothioate--hydrogen iodide (1/1) | HCID 2775205 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178484946 | HCID 178484946 | — |
Reaction Steps
2-phenylethylamine (2.4 g.), N,N',S-trimethylisothiourea hydriodide (4.92 g.) and ethanol (70 ml.), were boiled together under reflux for eight hours; methyl mercaptan was evolved. The resulting solution was evaporated to dryness and the residue recrystallised from methanol/ether mixture to yield N,N'-dimethyl-N"-2-phenylethylguanidine hydriodide, melting point 156°-160°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03968243 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-f4ee57d54bcb4c648d3450532234631c |
| Source note | uspto-grants-1976_07 |