HCID 12279215, compound → HCID 131710391, compound

HRID 918062Notes

Reaction equation

HRID 918062 reaction equation
[Cl:1]C1C=CC2N(C)C(=O)[CH2:9][N:8]3C=NN=[C:7]3[C:6]=2[CH:17]=1.[Cl:18][C:19]1[CH:20]=[CH:21][C:22]2[N:28]([CH3:29])[C:27](=[O:30])[CH2:26][N:25]3[C:31](C(F)(F)F)=[N:32][N:33]=[C:24]3[C:23]=2[CH:38]=1>>[ClH:1].[Cl:18][C:19]1[CH:20]=[CH:21][C:22]([NH:28][CH3:29])=[C:23]([C:24]2[N:25]([CH2:26][C:27](=[O:30])[N:8]3[CH2:7][CH2:6][CH2:17][CH2:9]3)[CH:31]=[N:32][N:33]=2)[CH:38]=1

Participants

3

Reactant 2

HCID 12279215HCID 12279215, compoundHCID 12279219HCID 12279219, compound

Product 1

HCID 131710391HCID 131710391, compound

Procedure

Following the procedure of example 1b but substituting an equivalent amount of 10-chloro-7-methyl-5H-s-triazolo[4,3-d]-[1,4]benzodiazepin-6(7H)-one for the 10-chloro-7-methyl-3-(trifluoromethyl)-5H-s-triazolo[4,3-d][1,4]benzodiazepin-6(7H)-one, one obtains the titled compound.

Sources & evidence

ORD record
ord-28e8049a53b34629abe8d3082293b683
Source dataset
uspto-grants-1976_07
Patent number
US03969366

Reaction notes

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