HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methyl-2-thiophenecarboxaldehyde → HCID 21436074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methyl-2-thiophenecarboxaldehyde | HCID 79911 | — |
| Reactant | 2-Amino-4-Nitrophenol | HCID 3613389 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21436074 | HCID 21436074 | 91.9% |
Reaction Steps
To a solution of 4-nitro-o-aminophenol (15.4 g, 0.1 mole) in 200 ml of ethanol, 3-methyl-2-thiophene carboxaldehyde (12.6 g, 0.1 mole) is added at room temperature. The mixture is allowed to stir for 1 hour and the precipitated yellow Schiff's Base is collected. Crystallization from acetonitrile yields 24.1 g of product, melting point 169°-171°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03969351 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-92036d1fcaf64bf29dc56309687528e7 |
| Source note | uspto-grants-1976_07 |