Urea, (1-methylcyclohexyl)- → HCID 21487893, compound

HRID 918078Notes

Reaction equation

HRID 918078 reaction equation
[O:1]1[CH2:5][C:4](=O)[CH2:3][C:2]1=[O:7].[CH3:8][C:9]1([NH:15][C:16]([NH2:18])=[O:17])[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1>>[CH3:8][C:9]1([NH:15][C:16]([NH:18][C:4]2[CH2:5][O:1][C:2](=[O:7])[CH:3]=2)=[O:17])[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1

Participants

3

Reactant 2

HCID 199098Urea, (1-methylcyclohexyl)-HCID 521261Tetronic acid

Product 1

HCID 21487893HCID 21487893, compoundYield 38.2%

Procedure

Using the procedure described in Example 2 using 5 g of 2,4-furandione and 6 g of 1-methylcyclohexylurea there is obtained 3.5 g 1-(1-methylcyclohexyl)-3-(2,5-dihydro-5-oxo-3-furyl)urea, m.p. 183°C. (decomposition).

Sources & evidence

ORD record
ord-4a3cdc233f8f4e94a9534272c25937e6
Source dataset
uspto-grants-1976_07
Patent number
US03969370

Reaction notes

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