HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Dioxide → Ethyl 2-methyl-1,3-benzodioxole-2-ethanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Dioxide | HCID 280 | — |
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | HCID 13269093 | HCID 13269093 | — |
| Product | Ethyl 2-methyl-1,3-benzodioxole-2-ethanoate | HCID 231059 | — |
Reaction Steps
13 g of ethyl acetoacetate and 13.6 g of pyrocatechol carbonate are heated until evolution of CO2 ceases. The residue is distilled under reduced pressure, b.p. 83°-86°C/0.3 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03969368 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-bb9914560de7476da10f03d4d2fd5e08 |
| Source note | uspto-grants-1976_07 |