HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → Dec-2-YN-1-YL 7-cyclopropylheptanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2-Decyn-1-ol | HCID 77763 | — |
| Reactant | 7-Cyclopropylheptanoyl chloride | HCID 21489670 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | Dec-2-YN-1-YL 7-cyclopropylheptanoate | HCID 21522904 | — |
Reaction Steps
To 60 ml. anhydrous ether and 1.5 g. 7-cyclopropylheptanoyl chloride is added 1.2 g. 2-decyn-1-ol. The mixture is cooled to 0° and 0.8 ml. pyridine is added. The solution is stirred at room temperature for 1 day. The product is worked up using the procedure of Example 1C to yield 2-decynyl 7-cyclopropylheptanoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03969384 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-b6fd8f9e5d76496d92069b0db6a0a953 |
| Source note | uspto-grants-1976_07 |