Sulfuric Acid → HCID 54391296, compound

Participants

Reaction Steps

The procedure described in Example 11 is repeated except that 10 g of 1-phenyl-2-(N-benzyl)amino-3-hydroxy-3,4-dimethyl-6-methoxyhexane obtained according to the procedure described in Example 5 is used in place of 1-(p-methoxy)phenyl-2-(N-benzyl)amino-3-hydroxy-3,4-dimethyl-6-methoxyhexane and 95% sulfuric acid is used in place of 93% sulfuric acid. As the result, 6 g of 1-phenyl-2-(N-benzyl)amino-3,4-dimethyl-6-methoxy-3-hexene is obtained as fractions having a boiling point of 191° - 196°C/1 mm Hg.

Provenance & Evidence