HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Toluenesulfonyl chloride → 1,6-Diisocyanohexane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Toluenesulfonyl chloride | HCID 7397 | — |
| Reactant | N-(6-formamidohexyl)formamide | HCID 252508 | — |
| Product | 1,6-Diisocyanohexane | HCID 3391105 | — |
Reaction Steps
1,6-diisocyanohexane was prepared by dehydration of N,N'-diformyl-(1,6-diaminohexane) with p-toluene sulfonyl chloride, essentially as described by Heztler and Covey (N. R. Heztler and E. J. Corey (1918), J. Org. Chem. 23 1222).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03970597 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-ee13330ab1e84a6f8b8dcbd6ea9fb9f6 |
| Source note | uspto-grants-1976_07 |