HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → [(1R,5S)-5-Hydroxycyclopent-2-en-1-yl]acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Ethyl ortho-acetate | HCID 86598186 | — |
| Product | [(1R,5S)-5-Hydroxycyclopent-2-en-1-yl]acetic acid | HCID 12813247 | — |
Reaction Steps
In the same manner as described in Example 1 but using 0.5 part of phenol in place of the hydroquinone, 7 parts of unreacted ethyl orthoacetate was recovered and then 4.2 parts of the desired product, a lactone of cis-2-hydroxy-cyclopent-4-ene-1-acetic acid was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03970673 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-36670f1655184ab0bbbbec30f7e23d1f |
| Source note | uspto-grants-1976_07 |