HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 53770322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 53977052 | HCID 53977052 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 53770322 | HCID 53770322 | — |
Reaction Steps
One gram of 3,7,11-trimethyltrideca-2,4,10-trienoic acid in 30 ml. of benzene and one mol of sodium hydride is stirred about two hours and then a slight excess of oxalyl chloride is added at about 0° and stirred for one hour. The product is worked up by removal of solvent in vacuo and extraction with pentane to yield 3,7,11-trimethyltrideca-2,4,10-trienoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03970704 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-1cde53a0c898410185fec8760577462f |
| Source note | uspto-grants-1976_07 |