HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanediamine → 2-(Nitromethylidene)-1-(prop-2-en-1-yl)hexahydropyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanediamine | HCID 428 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | Pyrimidine, hexahydro-2-(nitromethylene)- | HCID 11789315 | — |
| Product | 2-(Nitromethylidene)-1-(prop-2-en-1-yl)hexahydropyrimidine | HCID 70638990 | — |
Reaction Steps
Method B, reacting hexahydro-2-(nitromethylene)pyrimidine (HNMP), prepared by Method A by reaction of NKDM with 1,3-propanediamine, with allyl bromide. Melting point: 125°-126°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03971774 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-ecd18dd4ddd7490a9bbd149b861f92b1 |
| Source note | uspto-grants-1976_07 |