Crotyl chloride → 1-(But-2-en-1-yl)-2-(nitromethylidene)imidazolidine

HRID 918364Notes

Reaction equation

[N+:1]([CH:4]=[C:5]1[NH:9][CH2:8][CH2:7][NH:6]1)([O-:3])=[O:2].Cl[CH2:11][CH:12]=[CH:13][CH3:14]>>[CH2:11]([N:6]1[CH2:7][CH2:8][NH:9][C:5]1=[CH:4][N+:1]([O-:3])=[O:2])[CH:12]=[CH:13][CH3:14]

Participants

Reactant 2

HCID 11589Crotyl chloride

HCID 30147632-(Nitromethylene)imidazolidine

Product 1

HCID 706388111-(But-2-en-1-yl)-2-(nitromethylidene)imidazolidine

Procedure

Method B, 2-(nitromethylene)imidazolidine was reacted with 1-chloro-2-butene. Melting point: 82°-85°.

Sources & evidence

ORD record: ord-402e6f3159d54825962d81e5a007b44f
Source dataset: uspto-grants-1976_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03971774

Reaction notes

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