HRID918537

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID10434

1,3-Cyclohexanedione

C6H8O2

HCID4599837

Carbamimidoyl-acetic acid ethyl ester

C5H10N2O2

HCID11084437

Ethyl 3-formylbenzoate

C10H10O3

PRODUCTS

生成物

结构：CCOC(=O)C1=C(N)NC2=C(C(=O)CCC2)C1c1cccc(C(=O)OCC)c1

HCID12391116

未命名化合物

收率 54%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

2 次

PROCEDURE

实验过程

Upon heating a solution of 8.9 g of 3-carbethoxybenzaldehyde, 5.6 g of cyclohexane-1,3-dione and 6.5 g of amidinoacetic acid ethyl ester in 100 ml of ethanol for 4 hours, 2-amino-4-(3-carbethoxyphenyl)-1,4,5,6,7,8-hexahydro-5-oxoquinoline-3-carboxylic acid ethyl ester of melting point 234°C (ethanol) is obtained. Yield: 54% of theory.