HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 20330524, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 20330492 | HCID 20330492 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 20330524 | HCID 20330524 | — |
Reaction Steps
To a solution of 0.1 mole of 3-ethoxycarbonyloxy-4-ethoxycarbonyloxymethyl-5-hydroxymethyl-2-methylpyridine in 200 ml. of benzene is added dropwise with stirring and cooling 0.15 moles of thionyl chloride. The reaction mixture is stirred for 1 hour and then filtered to give 5-chloromethyl-3-ethoxycarbonyloxy-4-ethoxycarbonyloxymethyl-2-methylpyridine hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03971797 |
| Source dataset | uspto-grants-1976_07 |
| ORD ID | ord-4242bdffa2c446f18da0b615d4f94125 |
| Source note | uspto-grants-1976_07 |